C₃₇H₄₂N₄O₂Si

Base Information

Chemical Name:C₃₇H₄₂N₄O₂Si
CAS No.:1394130-37-0
Molecular Formula:C₃₇H₄₂N₄O₂Si
Molecular Weight:602.852
Hs Code.:

C<sub>37</sub>H<sub>42</sub>N<sub>4</sub>O<sub>2</sub>Si

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Chemical Property of C₃₇H₄₂N₄O₂Si

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Technology Process of C₃₇H₄₂N₄O₂Si

There total 9 articles about C₃₇H₄₂N₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1394130-36-9
C₃₀H₃₈N₄OSi

: 90-02-8
salicylaldehyde

: 1394130-37-0
C₃₇H₄₂N₄O₂Si

Guidance literature:: In methanol; for 2h; Reflux;
DOI:10.1039/c2cc34159j

Reference yield:

: C₃₄H₄₆N₂O₃Si

: 1394130-37-0
C₃₇H₄₂N₄O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / 20 °C

2: hydrazine hydrate / ethanol / 2 h / Reflux

3: methanol / 2 h / Reflux

With hydrazine hydrate; trifluoroacetic acid; In methanol; ethanol;
DOI:10.1039/c2cc34159j

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1394130-37-0
C₃₇H₄₂N₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 12 h / -78 - 20 °C / Inert atmosphere

3.1: sec.-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 - 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / 20 °C

5.1: hydrazine hydrate / ethanol / 2 h / Reflux

6.1: methanol / 2 h / Reflux

With n-butyllithium; oxalyl dichloride; hydrazine hydrate; sec.-butyllithium; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1039/c2cc34159j