Technology Process of C29H27F3N4O4
There total 12 articles about C29H27F3N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran
2.1: sodium tetrahydroborate
2.2: Reflux
3.1: toluene-4-sulfonic acid / dichloromethane
4.1: potassium carbonate / acetonitrile
5.1: hydrogen; palladium 10% on activated carbon; acetic acid
6.1: N-ethyl-N,N-diisopropylamine
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2015.01.066
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / dichloromethane
2: potassium carbonate / acetonitrile
3: hydrogen; palladium 10% on activated carbon; acetic acid
4: N-ethyl-N,N-diisopropylamine
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2015.01.066
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate
1.2: Reflux
2.1: toluene-4-sulfonic acid / dichloromethane
3.1: potassium carbonate / acetonitrile
4.1: hydrogen; palladium 10% on activated carbon; acetic acid
5.1: N-ethyl-N,N-diisopropylamine
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2015.01.066
