Technology Process of C19H21N3O2
There total 4 articles about C19H21N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C17H19N3O; acetic anhydride;
With
triethylamine;
In
dichloromethane;
at 20 - 25 ℃;
for 16h;
Inert atmosphere;
With
ammonia;
In
methanol; dichloromethane;
at 20 - 25 ℃;
for 144h;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bis(triphenylphosphine)palladium(II)-chloride; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / 80 °C / Inert atmosphere
2.1: ammonia / methanol / 16 h / 20 - 25 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 16 h / 20 - 25 °C / Inert atmosphere
3.2: 144 h / 20 - 25 °C
With
bis(triphenylphosphine)palladium(II)-chloride; ammonia; sodium carbonate; triethylamine;
In
methanol; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ammonia / methanol / 16 h / 20 - 25 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 16 h / 20 - 25 °C / Inert atmosphere
2.2: 144 h / 20 - 25 °C
With
ammonia; triethylamine;
In
methanol; dichloromethane;
DOI:10.1021/jm3011349