2-iodo-3-methyl-4-nitrobenzoic acid

Base Information

Chemical Name:2-iodo-3-methyl-4-nitrobenzoic acid
CAS No.:947690-07-5
Molecular Formula:C₈H₆INO₄
Molecular Weight:307.044
Hs Code.:

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Chemical Property of 2-iodo-3-methyl-4-nitrobenzoic acid

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Technology Process of 2-iodo-3-methyl-4-nitrobenzoic acid

There total 5 articles about 2-iodo-3-methyl-4-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 332082-31-2
2-amino-3-methyl-4-nitrobenzoic acid

: 947690-07-5
2-iodo-3-methyl-4-nitrobenzoic acid

Guidance literature:: 2-amino-3-methyl-4-nitrobenzoic acid; With phosphoric acid; sulfuric acid; sodium nitrite; at 5 - 10 ℃; for 0.5h;

With copper(l) iodide; potassium iodide; at 80 ℃; for 0.166667h; Further stages.;
DOI:10.1021/jm0702175

Reference yield:

: C₁₃H₁₄N₂O₇

: 947690-07-5
2-iodo-3-methyl-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: aq. NH₂OH*HCl / ethanol / 1.5 h / Heating

2.1: aq. H₂SO₄ / 2.5 h / 93 °C

3.1: aq. H₂O₂; KOH; KCl / 2 h / 20 °C

4.1: NaNO₂; aq. H₂SO₄; H₃PO₄ / 0.5 h / 5 - 10 °C

4.2: aq. KI; CuI / 0.17 h / 80 °C

With potassium hydroxide; phosphoric acid; sulfuric acid; potassium chloride; hydroxylamine hydrochloride; dihydrogen peroxide; sodium nitrite; In ethanol;
DOI:10.1021/jm0702175

Reference yield:

: 603-83-8
3-nitro-o-tolylamine

: 947690-07-5
2-iodo-3-methyl-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: KHCO₃ / CH₂Cl₂ / 1 h / 20 °C

2.1: aq. NH₂OH*HCl / ethanol / 1.5 h / Heating

3.1: aq. H₂SO₄ / 2.5 h / 93 °C

4.1: aq. H₂O₂; KOH; KCl / 2 h / 20 °C

5.1: NaNO₂; aq. H₂SO₄; H₃PO₄ / 0.5 h / 5 - 10 °C

5.2: aq. KI; CuI / 0.17 h / 80 °C

With potassium hydroxide; phosphoric acid; sulfuric acid; potassium chloride; hydroxylamine hydrochloride; dihydrogen peroxide; potassium hydrogencarbonate; sodium nitrite; In ethanol; dichloromethane;
DOI:10.1021/jm0702175