C₂₆H₂₈N₂O₃

Base Information

Chemical Name:C₂₆H₂₈N₂O₃
CAS No.:1426235-83-7
Molecular Formula:C₂₆H₂₈N₂O₃
Molecular Weight:416.52
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₆H₂₈N₂O₃

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Technology Process of C₂₆H₂₈N₂O₃

There total 16 articles about C₂₆H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426235-82-6
C₂₈H₃₃N₃O₄

: 1426235-83-7
C₂₆H₂₈N₂O₃

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; at -78 - 10 ℃; for 3.5h;
DOI:10.1016/j.tetlet.2013.01.074

Reference yield:

: 154-09-6,526-53-4,2899-29-8,52485-52-6
L-tryptophanol

: 1426235-83-7
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: p-toluenesulfonyl chloride; pyridine / 16 h / 0 - 20 °C

1.2: 2 h / 65 °C

1.3: 0.5 h / -78 °C

2.1: dichloromethane / 16 h / 20 °C / Molecular sieve

2.2: 6 h / -78 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 40 h / 80 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

6.1: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / 0.25 h / -60 - 20 °C

7.1: dichloromethane / 5 h / 0 - 20 °C

8.1: n-butyllithium; diethylamine / tetrahydrofuran / 2 h / -78 °C

9.1: lithium borohydride / tetrahydrofuran / 16 h / 66 °C

10.1: toluene-4-sulfonic acid / tetrahydrofuran / 16 h / 66 °C

11.1: 20% palladium hydroxide-activated charcoal; hydrogen / 2,2,2-trifluoroethanol / 16 h / 20 °C

12.1: triethylamine / dichloromethane / 16 h / 20 °C

13.1: trimethylaluminum / dichloromethane / 16 h / 20 °C

14.1: sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C

15.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 3.5 h / -78 - 10 °C

With pyridine; lithium aluminium tetrahydride; lithium borohydride; n-butyllithium; oxalyl dichloride; 20% palladium hydroxide-activated charcoal; tetrabutyl ammonium fluoride; hydrogen; trimethylaluminum; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide; acetonitrile; 2.1: |Pictet-Spengler Synthesis / 2.2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.tetlet.2013.01.074

Reference yield:

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 1426235-83-7
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C

2.1: p-toluenesulfonyl chloride; pyridine / 16 h / 0 - 20 °C

2.2: 2 h / 65 °C

2.3: 0.5 h / -78 °C

3.1: dichloromethane / 16 h / 20 °C / Molecular sieve

3.2: 6 h / -78 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 40 h / 80 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

7.1: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / 0.25 h / -60 - 20 °C

8.1: dichloromethane / 5 h / 0 - 20 °C

9.1: n-butyllithium; diethylamine / tetrahydrofuran / 2 h / -78 °C

10.1: lithium borohydride / tetrahydrofuran / 16 h / 66 °C

11.1: toluene-4-sulfonic acid / tetrahydrofuran / 16 h / 66 °C

12.1: 20% palladium hydroxide-activated charcoal; hydrogen / 2,2,2-trifluoroethanol / 16 h / 20 °C

13.1: triethylamine / dichloromethane / 16 h / 20 °C

14.1: trimethylaluminum / dichloromethane / 16 h / 20 °C

15.1: sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C

16.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 3.5 h / -78 - 10 °C

With pyridine; lithium aluminium tetrahydride; lithium borohydride; n-butyllithium; oxalyl dichloride; 20% palladium hydroxide-activated charcoal; tetrabutyl ammonium fluoride; hydrogen; trimethylaluminum; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide; acetonitrile; 3.1: |Pictet-Spengler Synthesis / 3.2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.tetlet.2013.01.074