32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

Base Information

Chemical Name:32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid
CAS No.:1341223-27-5
Molecular Formula:C₅₀H₆₇FN₆O₁₄
Molecular Weight:994.114
Hs Code.:

32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

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Chemical Property of 32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

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Technology Process of 32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

There total 14 articles about 32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255942-02-9
N-[6-(6H-dibenzo[b,f]azocin-5-yl)-6-oxo-hexyl]-2,2,2-trifluoroacetamide

: 1341223-27-5
32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

: C₅₀H₆₇⁽¹⁸⁾FN₆O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium hydrobromide perbromide; potassium tert-butylate

2: potassium carbonate / methanol / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 37 °C

4: N,N-dimethyl-formamide / 0.5 h / 37 °C

With pyridinium hydrobromide perbromide; potassium tert-butylate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ml200187j

Reference yield:

: 124915-09-9
ethyl 4-[18F]fluorobenzoate

: 1341223-27-5
32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

: C₅₀H₆₇⁽¹⁸⁾FN₆O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1: water; sodium hydroxide

2: trimethylammonium hydroxide / water; acetonitrile / 0.08 h / 100 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 37 °C

4: N,N-dimethyl-formamide / 0.5 h / 37 °C

With trimethylammonium hydroxide; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ml200187j

Reference yield:

: 1255942-04-1
N-(6-trifluoroacetamidohexanoyl)-5,6-dihydro-11,12-didehydrodibenzo[b,f]azocine

: 1341223-27-5
32-(8-(6-(4-[18F]fluorobenzamido)hexanoyl)-8,9-dihydro-1H-dibenzo[b,f][1,2,3]triazolo-[4,5-d]azocin-1-yl)-5-oxo-3,9,12,15,18,21,24,27,30-nonaoxa-6-azadotriacontan-1-oic acid

: C₅₀H₆₇⁽¹⁸⁾FN₆O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 37 °C

3: N,N-dimethyl-formamide / 0.5 h / 37 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ml200187j