tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene)

Base Information

Chemical Name:tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene)
CAS No.:102744-55-8
Molecular Formula:C₄H₁₂N*C₁₆H₁₆B
Molecular Weight:293.26
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene)

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Technology Process of tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene)

There total 1 articles about tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 89377-15-1
1-phenyl-2-borolene

: 64-20-0
tetramethylammonium bromide

: 591-51-5
phenyllithium

: 102744-55-8
tetramethylammonium-(1,1-diphenyl-borata-2-cyclopentene)

Guidance literature:: In diethyl ether; (N2) or (Ar); addn. of 1-phenyl-2-borolene to LiPh at 0°C under stirring; stirring for 10 min at room temp.; evapn. of solvent; shaking residue with water; addn. of (NMe4)Br; filtration; washing with H2O, EtOH and Et2O; recrystn. from acetone/Et2O; elem. anal.;