symplocamide A

Base Information

Chemical Name:symplocamide A
CAS No.:1007391-44-7
Molecular Formula:C₄₆H₇₁BrN₁₀O₁₃
Molecular Weight:1052.03
Hs Code.:

Synonyms:

Suppliers and Price of symplocamide A

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of symplocamide A

Chemical Property:

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Technology Process of symplocamide A

There total 2 articles about symplocamide A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 1260112-34-2
(S)-3-(3-bromo-4-methoxyphenyl)-2-((N-tert-butoxycarbonyl)-(methyl)amino)propanoic acid

: (S)-9-(allyloxy)-8-[bis((tert-butoxy)carbonyl)amino]-9-oxonon-4-enoic acid

: 13726-85-7
Boc-Gln-OH

: 68858-20-8
Fmoc-Val-OH

: 71989-23-6,251316-98-0
Fmoc-Ile-OH

: 73731-37-0
Fmoc-Thr-OH

: 133174-15-9
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-ureidopentanoic acid

: 107-92-6
butyric acid

: 1007391-44-7
symplocamide A

Guidance literature:: (S)-9-(allyloxy)-8-[bis((tert-butoxy)carbonyl)amino]-9-oxonon-4-enoic acid; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 24.5h; Inert atmosphere; solid phase reaction;

With trifluoroacetic acid; In dichloromethane; for 1.08333h; solid phase reaction;

(S)-3-(3-bromo-4-methoxyphenyl)-2-((N-tert-butoxycarbonyl)-(methyl)amino)propanoic acid; Boc-Gln-OH; Fmoc-Val-OH; Fmoc-Ile-OH; Fmoc-Thr-OH; (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-ureidopentanoic acid; butyric acid; Further stages;
DOI:10.1039/c0cc02889d

Reference yield:

: C₅₀H₇₇BrN₁₁O₁₃Pol

: 1007391-44-7
symplocamide A

Guidance literature:: C₅₀H₇₇BrN₁₁O₁₃Pol; With 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate; In tetrahydrofuran; water; for 0.166667h; solid phase reaction;

With osmium(VIII) oxide; In tetrahydrofuran; water; tert-butyl alcohol; for 20h;
DOI:10.1002/ejoc.201101757