1-(3-HCCC₆H₄)-1,2-C₂B₁₀H₁₁

Base Information

• Chemical Name: 1-(3-HCCC₆H₄)-1,2-C₂B₁₀H₁₁
• CAS No.: 1070719-97-9
• Molecular Formula: C₁₀H₁₆B₁₀
• Molecular Weight: 244.347
• Mol file: 1070719-97-9.mol

Synonyms:

Chemical Property of 1-(3-HCCC₆H₄)-1,2-C₂B₁₀H₁₁

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-(3-HCCC₆H₄)-1,2-C₂B₁₀H₁₁

There total 1 articles about 1-(3-HCCC₆H₄)-1,2-C₂B₁₀H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

nido-decaborane (17702-41-9) + 1,3-diethynylbenzene (1785-61-1) → 1-(3-HCCC6H4)-1,2-C2B10H11 (1070719-97-9)

Guidance literature:

With 1-butyl-3-methylimidazolium chloride; In further solvent(s); byproducts: H2; under Ar; B10H14 and C6H4(CCH)2 (molar ratio 1:1.6) in biphasic toluene - 1-butyl-3-methylimidazolium chloride stirred at 120°C for ca. 20 min; top org. layer sepd. by pipette; ionic liq. layer extd. with ether; combined toluene and ether extracts vac. concd.; flash filtered (silica gel column, hexanes); elem. anal.;

DOI:10.1021/ic800999y

upstream raw materials:

nido-decaborane

1,3-diethynylbenzene