Technology Process of C45H44N12O8S5
There total 7 articles about C45H44N12O8S5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
dichloromethane; water; acetonitrile;
at 20 ℃;
for 72h;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 6 steps
1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2: triethylamine / acetone / Sonication
3: sodium azide / acetone / 1.33 h / 60 °C
4: 14 h / 80 °C
5: trifluoroacetic acid / dichloromethane / 2 h
6: caesium carbonate / dichloromethane; water; acetonitrile / 72 h / 20 °C
With
sodium azide; water; caesium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
4: Curtius rearrangement;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 7 steps
1: formic acid
2: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
3: triethylamine / acetone / Sonication
4: sodium azide / acetone / 1.33 h / 60 °C
5: 14 h / 80 °C
6: trifluoroacetic acid / dichloromethane / 2 h
7: caesium carbonate / dichloromethane; water; acetonitrile / 72 h / 20 °C
With
formic acid; sodium azide; water; caesium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
5: Curtius rearrangement;
DOI:10.1021/jm101602q
