benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

Base Information

Chemical Name:benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate
CAS No.:1303609-24-6
Molecular Formula:C₁₉H₃₁NO₃Si
Molecular Weight:349.546
Hs Code.:

Synonyms:

Suppliers and Price of benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

There total 1 articles about benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Chloressigsaeure-ethylester

: 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutanecarboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1303609-24-6
benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

: 1303609-23-5
benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

Guidance literature:: Chloressigsaeure-ethylester; 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutanecarboxylic acid; With triethylamine; In acetone; at 0 ℃; for 0.5h;

With sodium azide; In water; acetone; at 0 ℃; for 0.333333h;

benzyl alcohol; In toluene; at 80 ℃; for 2h; Overall yield = 1.03 g;
DOI:10.1021/ja3125417

Reference yield:

: 1303609-24-6
benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

: 1303609-29-1
MI-519-65-TFA

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; sodium hydrogencarbonate / palladium on activated charcoal / isopropyl alcohol / 1 h / 760.05 Torr

2.1: tetrahydrofuran

2.2: 0.5 h

3.1: hydrogenchloride / methanol; water / 1 h / 20 °C

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water; isopropyl alcohol;

Reference yield:

: 1303609-24-6
benzyl 3-(tert-butyldimethylsilyloxy)-3-methylcyclobutylcarbamate

: 1303609-28-0
C₄₈H₅₈Cl₂FN₃O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen; sodium hydrogencarbonate / palladium on activated charcoal / isopropyl alcohol / 1 h / 760.05 Torr

2.1: tetrahydrofuran

2.2: 0.5 h

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; isopropyl alcohol;