Technology Process of C24H40O5Si
There total 6 articles about C24H40O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tert-butyldimethylsilyl chloride; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C
2: potassium carbonate / acetone / 2 h / 55 °C
With
potassium carbonate; tert-butyldimethylsilyl chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; acetone;
1: |Claisen-Ireland Rearrangement;
DOI:10.5012/bkcs.2013.34.7.1949
- Guidance literature:
-
Multi-step reaction with 5 steps
1: CSA / water; methanol
2: triethylamine / dichloromethane
3: triethylamine; dmap / dichloromethane
4: tert-butyldimethylsilyl chloride; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C
5: potassium carbonate / acetone / 2 h / 55 °C
With
dmap; potassium carbonate; tert-butyldimethylsilyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone;
4: |Claisen-Ireland Rearrangement;
DOI:10.5012/bkcs.2013.34.7.1949
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diisobutylaluminium hydride / dichloromethane / -78 °C
2: sodium hydride / tetrahydrofuran
3: CSA / water; methanol
4: triethylamine / dichloromethane
5: triethylamine; dmap / dichloromethane
6: tert-butyldimethylsilyl chloride; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C
7: potassium carbonate / acetone / 2 h / 55 °C
With
dmap; sodium hydride; diisobutylaluminium hydride; potassium carbonate; tert-butyldimethylsilyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone;
6: |Claisen-Ireland Rearrangement;
DOI:10.5012/bkcs.2013.34.7.1949