C₁₂H₇N₂PS₃

Base Information

Chemical Name:C₁₂H₇N₂PS₃
CAS No.:1443540-68-8
Molecular Formula:C₁₂H₇N₂PS₃
Molecular Weight:306.373
Hs Code.:

C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>PS<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₂H₇N₂PS₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₇N₂PS₃

Chemical Property:

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Technology Process of C₁₂H₇N₂PS₃

There total 3 articles about C₁₂H₇N₂PS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1443540-65-5
C₁₂H₇N₂PS₂

: 1443540-68-8
C₁₂H₇N₂PS₃

Guidance literature:: With sulfur; In toluene; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1002/chem.201204375

Reference yield:

: 1443540-64-4
C₃₀H₄₇N₂PS₂Si₂

: 1443540-68-8
C₁₂H₇N₂PS₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: sulfur / toluene / Inert atmosphere; Schlenk technique; Reflux

With tetrabutyl ammonium fluoride; sulfur; In tetrahydrofuran; toluene;
DOI:10.1002/chem.201204375

Reference yield:

: 1223559-98-5
4,4′-dibromo-2,2′-bis(triisopropylsilanyl)[5,5′]bithiazolyl

: 1443540-68-8
C₁₂H₇N₂PS₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

3.1: sulfur / toluene / Inert atmosphere; Schlenk technique; Reflux

With n-butyllithium; tetrabutyl ammonium fluoride; sulfur; In tetrahydrofuran; diethyl ether; hexane; toluene;
DOI:10.1002/chem.201204375