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Technology Process of C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4

C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4

Base Information
  • Chemical Name:C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4
  • CAS No.:110282-27-4
  • Molecular Formula:C24H32CoCrO5PS
  • Molecular Weight:574.544
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>Co(P(CH<sub>3</sub>)3)S(Cr(CO)5)CC<sub>6</sub>H<sub>6</sub>(CH<sub>3</sub>)4

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Chemical Property of C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4
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Technology Process of C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4

There total 1 articles about C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

(cyclopentadienyl)(1,1,3,3-tetramethyl-2-thiocarbonylcyclohexan)(trimethylphosphan)cobalt

(cyclopentadienyl)(1,1,3,3-tetramethyl-2-thiocarbonylcyclohexan)(trimethylphosphan)cobalt

chromium<sup>(0)</sup> hexacarbonyl
199620-14-9,13007-92-6

chromium(0) hexacarbonyl

C<sub>5</sub>H<sub>5</sub>Co(P(CH<sub>3</sub>)3)S(Cr(CO)5)CC<sub>6</sub>H<sub>6</sub>(CH<sub>3</sub>)4
110282-27-4

C5H5Co(P(CH3)3)S(Cr(CO)5)CC6H6(CH3)4

Guidance literature:
With THF; In tetrahydrofuran; Irradiation (UV/VIS); (N2), soln. of the Cr-complex irradiated for 8h, N2 occasionally bubbled through the soln., Co-complex added, stirred overnight at 20°C; evapd. to dryness in vacuo, toluene added, chromd. (silica gel/toluene), starting compd. eluted with acetone, volume of the soln. (2.fraction) reduced, filtered, pentane added, cooled to -35°C, elem. anal.;
DOI:10.1016/0022-328X(86)80457-0
upstream raw materials:

chromium(0) hexacarbonyl

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