N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane

Base Information

• Chemical Name: N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane
• CAS No.: 1206187-27-0
• Molecular Formula: C₆₄H₉₂N₂O₈
• Molecular Weight: 1017.44
• Mol file: 1206187-27-0.mol

Synonyms:

Chemical Property of N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane

There total 1 articles about N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,12-Diaminododecane (2783-17-7,95931-03-6) + 4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde (868620-29-5) → N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane (1206187-27-0)

Guidance literature:

In methanol; for 4h; Reflux;

DOI:10.1080/15421400802714098

Reference yield: 76.0%

N,N'-bis[4-(4-(dodecyloxy)benzoyloxy)-2-hydroxybenzylidene]-1,12-diaminododecane (1206187-27-0) + zinc(II) acetate dihydrate (5970-45-6) → (N,N'-bis[(4'-dodecyloxy)benzoyloxybenzylidene]-1,10-diaminododecane)zinc(II) (1224923-29-8)

Guidance literature:

In ethanol; Zn salt added to a hot soln. of ligand (1:10) in EtOH, stirred at refluxfor 5 h; cooled to room temp., filtered, recrystd.(CH3CN/CHCl3), dried (vac.), elem. anal.;

DOI:10.1002/ejic.200900536

upstream raw materials:

1,12-Diaminododecane

4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde

Downstream raw materials:

(N,N'-bis[(4'-dodecyloxy)benzoyloxybenzylidene]-1,10-diaminododecane)zinc(II)