Technology Process of C22H29NO2
There total 9 articles about C22H29NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Regis.(R). PIRKLE COVALENT (R,R) WHELK-01 / hexane; isopropyl alcohol / Resolution of racemate
2: chloroform / 6 h / -40 °C / Inert atmosphere; Irradiation
With
Regis PIRKLE COVALENT (R,R) WHELK-01;
In
hexane; chloroform; isopropyl alcohol;
DOI:10.1021/ja9050586
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / dichloromethane / 20 - 23 °C / Inert atmosphere
2: Regis.(R). PIRKLE COVALENT (R,R) WHELK-01 / hexane; isopropyl alcohol / Resolution of racemate
3: chloroform / 6 h / -40 °C / Inert atmosphere; Irradiation
With
sodium carbonate;
In
hexane; dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1021/ja9050586
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ethanol / 80 °C / Inert atmosphere
2: sodium tetrahydroborate / dimethyl sulfoxide / 80 °C / Inert atmosphere
3: sodium carbonate / dichloromethane / 20 - 23 °C / Inert atmosphere
4: Regis.(R). PIRKLE COVALENT (R,R) WHELK-01 / hexane; isopropyl alcohol / Resolution of racemate
5: chloroform / 6 h / -40 °C / Inert atmosphere; Irradiation
With
sodium tetrahydroborate; sodium carbonate;
In
ethanol; hexane; dichloromethane; chloroform; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/ja9050586
