2-benzylthio-UMP

Base Information

Chemical Name:2-benzylthio-UMP
CAS No.:1280117-19-2
Molecular Formula:C₁₆H₁₉N₂O₈PS
Molecular Weight:430.375
Hs Code.:

Synonyms:

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Chemical Property of 2-benzylthio-UMP

Chemical Property:

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Technology Process of 2-benzylthio-UMP

There total 7 articles about 2-benzylthio-UMP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1280116-91-7
2-benzylthio-1-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)pyrimidine-4-one

: 1280117-19-2
2-benzylthio-UMP

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; ammonia / 20 °C

2: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / triethyl phosphate / 5 h / Inert atmosphere; Cooling

3: water; triethylamine carbonate / 1 h / 20 °C / pH 7.4 - 7.6

With methanol; ammonia; water; triethylamine carbonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; In triethyl phosphate;
DOI:10.1021/jm1016297

Reference yield:

: 1280116-97-3
2-benzylthio-1-β-D-ribofuranosyl-pyrimidine-4-one

: 1280117-19-2
2-benzylthio-UMP

Guidance literature:: Multi-step reaction with 2 steps

1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / triethyl phosphate / 5 h / Inert atmosphere; Cooling

2: water; triethylamine carbonate / 1 h / 20 °C / pH 7.4 - 7.6

With water; triethylamine carbonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; In triethyl phosphate;
DOI:10.1021/jm1016297

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 1280117-19-2
2-benzylthio-UMP

Guidance literature:: Multi-step reaction with 6 steps

1: tin(IV) chloride / 1,2-dichloro-ethane / 7 h / 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / water; 1,2-dichloro-ethane / Inert atmosphere

3: triethylamine / dichloromethane / Reflux

4: methanol; ammonia / 20 °C

5: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / triethyl phosphate / 5 h / Inert atmosphere; Cooling

6: water; triethylamine carbonate / 1 h / 20 °C / pH 7.4 - 7.6

With methanol; ammonia; water; triethylamine carbonate; tin(IV) chloride; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydrogencarbonate; triethylamine; trichlorophosphate; In triethyl phosphate; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/jm1016297