Technology Process of C15H17N3O5
There total 5 articles about C15H17N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: H2 / Pd/C / methanol
1.2: tetrahydrofuran
2.1: 70 percent / tBuOK / tetrahydrofuran
3.1: 87 percent / tBuOK / tetrahydrofuran
4.1: TFA / CH2Cl2
4.2: isobutyl chloroformate; N-methylmorpholine
4.3: NH3 / tetrahydrofuran
With
potassium tert-butylate; hydrogen; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2007.03.066
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: TEA / silver benzoate
2.1: H2 / Pd/C / methanol
2.2: tetrahydrofuran
3.1: 70 percent / tBuOK / tetrahydrofuran
4.1: 87 percent / tBuOK / tetrahydrofuran
5.1: TFA / CH2Cl2
5.2: isobutyl chloroformate; N-methylmorpholine
5.3: NH3 / tetrahydrofuran
With
TEA; potassium tert-butylate; hydrogen; trifluoroacetic acid;
palladium on activated charcoal; silver benzoate;
In
tetrahydrofuran; methanol; dichloromethane;
1.1: Arndt-Eistert rearrangement;
DOI:10.1016/j.tetlet.2007.03.066
- Guidance literature:
-
C19H24N2O6;
With
trifluoroacetic acid;
In
dichloromethane;
With
4-methyl-morpholine; isobutyl chloroformate;
With
ammonia;
In
tetrahydrofuran;
Further stages.;
DOI:10.1016/j.tetlet.2007.03.066
