OMo(NNCPh₂)(S₂CNEt₂)2

Base Information

• Chemical Name: OMo(NNCPh₂)(S₂CNEt₂)2
• CAS No.: 100763-35-7
• Molecular Formula: C₂₃H₃₀MoN₄OS₄
• Molecular Weight: 602.721
• Mol file: 100763-35-7.mol

Synonyms:

Chemical Property of OMo(NNCPh₂)(S₂CNEt₂)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of OMo(NNCPh₂)(S₂CNEt₂)2

There total 1 articles about OMo(NNCPh₂)(S₂CNEt₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

bis(diethylcarbamodithioato-S,S')oxomolybdenum (63950-40-3,25395-92-0) + diazodiphenylmethane (908093-98-1) → OMo(NNCPh2)(S2CNEt2)2 (100763-35-7)

Guidance literature:

In tetrahydrofuran; Schlenk flask, N2-atmosphere, soln. of Mo-complex was cooled to -30°C, addn. of diazo compd. via cannula, warming to room temp. and stirring for 2h; vac., crystn. from toluene/pentane, recrystn. from toluene/ether, drying in vac.;

DOI:10.1021/om00113a031

Reference yield: 70.0%

OMo(NNCPh2)(S2CNEt2)2 (100763-35-7) + pentylidenetriphenylphosphorane (29541-98-8,55317-64-1) → Ph2CN2CH(CH2)3CH3 (122822-38-2)

Guidance literature:

In not given;

DOI:10.1021/om00113a031

upstream raw materials:

bis(diethylcarbamodithioato-S,S')oxomolybdenum

diazodiphenylmethane

Downstream raw materials:

Ph₂CN₂CH(CH₂)3CH₃