4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Base Information

Chemical Name:4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile
CAS No.:1235864-94-4
Molecular Formula:C₂₈H₁₉N₃
Molecular Weight:397.479
Hs Code.:

Synonyms:

Suppliers and Price of 4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

There total 4 articles about 4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 1235864-94-4
4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1 h / Cooling with ice

2.1: potassium acetate / palladium diacetate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / Reflux; Inert atmosphere

4.1: sodium hydride; methyl-triphenylphosphonium iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.2: 0.17 h / 0 °C / Cooling with ice

With N-Bromosuccinimide; potassium acetate; methyl-triphenylphosphonium iodide; sodium hydride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 56765-79-8
3,4-dicyanoaniline

: 1235864-94-4
4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / ethanol; water / 0.5 h / Cooling with ice

1.2: 20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / Reflux; Inert atmosphere

3.1: sodium hydride; methyl-triphenylphosphonium iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 0.17 h / 0 °C / Cooling with ice

With hydrogenchloride; methyl-triphenylphosphonium iodide; sodium hydride; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; water; toluene;

Reference yield:

: 847978-62-5
4-[N-(4-bromophenyl)-N-phenylamine]benzaldehyde

: 1235864-94-4
4'-(phenyl(4-vinylphenyl)amino)biphenyl-3,4-dicarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate / palladium diacetate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / Reflux; Inert atmosphere

3.1: sodium hydride; methyl-triphenylphosphonium iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 0.17 h / 0 °C / Cooling with ice

With potassium acetate; methyl-triphenylphosphonium iodide; sodium hydride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;