C₁₃H₁₂ClNS

Base Information

• Chemical Name: C₁₃H₁₂ClNS
• CAS No.: 1352622-28-6
• Molecular Formula: C₁₃H₁₂ClNS
• Molecular Weight: 249.764
• Mol file: 1352622-28-6.mol

Synonyms:

Chemical Property of C₁₃H₁₂ClNS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₂ClNS

There total 3 articles about C₁₃H₁₂ClNS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H10ClNO2S (1352622-72-0) → C13H12ClNS (1352622-28-6)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 75 ℃;

DOI:10.1021/ja2058583

Reference yield:

3-bromo-4-chloronitrobenzene (16588-26-4) → C13H12ClNS (1352622-28-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; quinoline / 2 h / 220 °C

2: iron; ammonium chloride / ethanol; water / 75 °C

With pyridine; quinoline; iron; ammonium chloride; In ethanol; water;

DOI:10.1021/ja2058583

Reference yield:

m-tolylthiolatocopper(I) (79161-38-9) → C13H12ClNS (1352622-28-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; quinoline / 2 h / 220 °C

2: iron; ammonium chloride / ethanol; water / 75 °C

With pyridine; quinoline; iron; ammonium chloride; In ethanol; water;

DOI:10.1021/ja2058583

upstream raw materials:

C₁₃H₁₀ClNO₂S

3-bromo-4-chloronitrobenzene

m-tolylthiolatocopper(I)

Refernces