Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-

Base Information

Chemical Name:Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-
CAS No.:110345-23-8
Molecular Formula:C₂₁H₁₄Cl₂N₄O
Molecular Weight:409.274
Hs Code.:
Mol file:110345-23-8.mol

Synonyms:BRN 5633215;1-(2,6-Dichlorophenyl)-3-(dimethylaminomethylene)-6-(dicyanoethylene)-indolin-2-one;Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-;110345-23-8

Suppliers and Price of Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-

Chemical Property:

Vapor Pressure:2.68E-14mmHg at 25°C
Boiling Point:598.8°C at 760 mmHg
Flash Point:315.9°C
Density:1.465g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:408.0544665
Heavy Atom Count:28
Complexity:759

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C=C1C2=C(C=C(C=C2)C=C(C#N)C#N)N(C1=O)C3=C(C=CC=C3Cl)Cl
Isomeric SMILES:CN(C)/C=C/1\C2=C(C=C(C=C2)C=C(C#N)C#N)N(C1=O)C3=C(C=CC=C3Cl)Cl

Technology Process of Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)-

There total 2 articles about Propanedinitrile, ((1-(2,6-dichlorophenyl)-3-((dimethylamino)methylene)-2,3-dihydro-2-oxo-1H-indol-6-yl)methylene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.5%

: 110326-34-6
1-(2,6-Dichlorophenyl)-3-(dimethylaminomethylene)-6-formylindolin-2-one

: 109-77-3
malononitrile

: 110345-23-8
1-(2,6-Dichlorophenyl)-3-(dimethylaminomethylene)-6-(dicyanoethylene)indolin-2-one

Guidance literature:: With piperidine; In ethanol; for 1h;
DOI:10.1007/BF00767397

Reference yield:

: 15362-40-0
1-(2,6-dichlorophenyl)indolin-2-one

: 110345-23-8
1-(2,6-Dichlorophenyl)-3-(dimethylaminomethylene)-6-(dicyanoethylene)indolin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 77.3 percent / POCl₃/DMF / CHCl₃ / 6 h

2: 36.5 percent / piperidine / ethanol / 1 h

With piperidine; N,N-dimethyl-formamide; trichlorophosphate; In ethanol; chloroform;
DOI:10.1007/BF00767397