Technology Process of C19H22O
There total 4 articles about C19H22O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 50 ℃;
for 2h;
DOI:10.1039/c1ob06189e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere
1.2: 80 °C / Inert atmosphere
2.1: t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); C26H27NO / toluene / 30 °C / Inert atmosphere
3.1: tert.-butyl lithium / diethyl ether; pentane / 2.5 h / -78 - 23 °C / Inert atmosphere
3.2: 2.42 h / -78 - 0 °C / Inert atmosphere
3.3: 0.33 h
4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 50 °C
With
hydrogenchloride; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); C26H27NO; tert.-butyl lithium; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; water; toluene; pentane;
3.2: Grignard reaction;
DOI:10.1039/c1ob06189e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); C26H27NO / toluene / 30 °C / Inert atmosphere
2.1: tert.-butyl lithium / diethyl ether; pentane / 2.5 h / -78 - 23 °C / Inert atmosphere
2.2: 2.42 h / -78 - 0 °C / Inert atmosphere
2.3: 0.33 h
3.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 50 °C
With
hydrogenchloride; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); C26H27NO; tert.-butyl lithium;
In
tetrahydrofuran; diethyl ether; water; toluene; pentane;
2.2: Grignard reaction;
DOI:10.1039/c1ob06189e
