C₂₉H₂₈N₂O₆S

Base Information

Chemical Name:C₂₉H₂₈N₂O₆S
CAS No.:1354014-48-4
Molecular Formula:C₂₉H₂₈N₂O₆S
Molecular Weight:532.617
Hs Code.:

C<sub>29</sub>H<sub>28</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₂₉H₂₈N₂O₆S

Chemical Property:

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Technology Process of C₂₉H₂₈N₂O₆S

There total 6 articles about C₂₉H₂₈N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354014-47-3
C₂₅H₂₄N₂O₄S

: 2937-50-0
Allyl chloroformate

: 1354014-48-4
C₂₉H₂₈N₂O₆S

: C₂₉H₂₈N₂O₆S

Guidance literature:: C₂₅H₂₄N₂O₄S; With n-butyllithium; (R,R)-N,N-bis-(1-phenylethyl)amine; lithium chloride; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

Allyl chloroformate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol203302f

Reference yield:

: C₂₇H₃₀N₂O₅S

: 1354014-48-4
C₂₉H₂₈N₂O₆S

: C₂₉H₂₈N₂O₆S

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium; (R,R)-N,N-bis-(1-phenylethyl)amine; lithium chloride / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: 12 h / -78 - 20 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; water; (R,R)-N,N-bis-(1-phenylethyl)amine; lithium chloride; In tetrahydrofuran; hexane;
DOI:10.1021/ol203302f

Reference yield:

: 1354014-34-8
C₂₂H₃₀N₂O₅

: 1354014-48-4
C₂₉H₂₈N₂O₆S

: C₂₉H₂₈N₂O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

1.2: 0.25 h / 0 °C / Inert atmosphere

2.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran; isopropyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium; (R,R)-N,N-bis-(1-phenylethyl)amine; lithium chloride / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

5.2: 12 h / -78 - 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; potassium tert-butylate; water; (R,R)-N,N-bis-(1-phenylethyl)amine; acetic acid; lithium chloride; In tetrahydrofuran; hexane; isopropyl alcohol; 1.1: Dieckmann reaction;
DOI:10.1021/ol203302f