W₂Cl₄(P(CH₃)2(C₆H₅))4

Base Information

Chemical Name:W₂Cl₄(P(CH₃)2(C₆H₅))4
CAS No.:147977-45-5
Molecular Formula:C₃₂H₄₄Cl₄P₄W₂
Molecular Weight:1062.11
Hs Code.:

W<sub>2</sub>Cl<sub>4</sub>(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>))4

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of W₂Cl₄(P(CH₃)2(C₆H₅))4

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Technology Process of W₂Cl₄(P(CH₃)2(C₆H₅))4

There total 1 articles about W₂Cl₄(P(CH₃)2(C₆H₅))4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13470-13-8
tungsten(IV) chloride

: 672-66-2
Dimethyl(phenyl)phosphine

: 73133-21-8,147977-45-5
W₂Cl₄(P(CH₃)2(C₆H₅))4

Guidance literature:: With sodium amalgam; In tetrahydrofuran; under N2 sodium amalgam and Me2PPh were added to THF at -30°C followed by WCl4; shaking and warming to room temp. for ca 0.5 h; decantation, filtration through Celite; evapn., extn. with pentane, filtration, evapn., washing with MeCN, drying in vac.; elem. anal.;

Reference yield:

: 73133-21-8,147977-45-5
W₂Cl₄(P(CH₃)2(C₆H₅))4

: W₂Cl₅(P(CH₃)2(C₆H₅))3

Guidance literature:: With (Dichloroiodo)benzene; In dichloromethane; Ar, vac. line or Schlenk techniques; org. oxidant addn. dropwise to equival. amt. of W-compd. soln.; gas chromy. mass spectrometry;
DOI:10.1016/0020-1693(95)04582-1