C₃₂H₅₄O₆Si

Base Information

Chemical Name:C₃₂H₅₄O₆Si
CAS No.:1416153-38-2
Molecular Formula:C₃₂H₅₄O₆Si
Molecular Weight:562.863
Hs Code.:

C<sub>32</sub>H<sub>54</sub>O<sub>6</sub>Si

Synonyms:

Suppliers and Price of C₃₂H₅₄O₆Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₂H₅₄O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₂H₅₄O₆Si

There total 20 articles about C₃₂H₅₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416153-34-8
(E)-3-[(1S,2R)-2-(triisopropylsilyloxy)cyclopent-1-yl]-3-propenal

: 1416153-38-2
C₃₂H₅₄O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; hexane / -70 °C

2: α,α,α-trifluorotoluene; magnesium oxide / 72 h / 85 °C

3: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 76 h / 20 °C

4: pyridine; dmap / 18 h / 20 °C / Cooling with ice

With pyridine; dmap; methanesulfonamide; α,α,α-trifluorotoluene; AD-mix-α; magnesium oxide; In tetrahydrofuran; hexane; water; tert-butyl alcohol;
DOI:10.1271/bbb.120317 DOI:10.1271/bbb.120317

Reference yield:

: 642454-37-3
(1S,2S)-2-(2-trityloxyethyl)cyclopentanol

: 1416153-38-2
C₃₂H₅₄O₆Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: triethylamine / dichloromethane; water / 1 h / 20 °C

2.1: dimethyl sulfoxide / 30 h / 60 °C

3.1: pyridinium p-toluenesulfonate / methanol / 4 h / Reflux

4.1: pyridinium chlorochromate / dichloromethane / 16 h / 20 °C / Molecular sieve

5.1: dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3 h / 20 °C

6.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; tert-butyl alcohol; acetone / 20 h / 20 °C

6.2: 4 h / 20 °C

7.1: pyridine / 16 h / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

9.1: sodium hydroxide / ethanol; water / 12 h / 60 °C

10.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 20 °C

11.1: formic acid / diethyl ether / -5 °C

12.1: pyridinium chlorochromate / dichloromethane; diethyl ether / 20 °C / Molecular sieve

13.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / -70 °C

13.2: -70 - 20 °C

14.1: acetic acid; water / tetrahydrofuran / 20 °C

15.1: tetrahydrofuran; hexane / -70 °C

16.1: α,α,α-trifluorotoluene; magnesium oxide / 72 h / 85 °C

17.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 76 h / 20 °C

18.1: pyridine; dmap / 18 h / 20 °C / Cooling with ice

With pyridine; 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; formic acid; methanesulfonamide; α,α,α-trifluorotoluene; AD-mix-α; water; pyridinium p-toluenesulfonate; magnesium oxide; potassium hexamethylsilazane; acetic acid; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; toluene; tert-butyl alcohol; 13.1: |Wittig-Horner Reaction;
DOI:10.1271/bbb.120317 DOI:10.1271/bbb.120317

Reference yield:

: C₂₇H₃₀O₄S

: 1416153-38-2
C₃₂H₅₄O₆Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: dimethyl sulfoxide / 30 h / 60 °C

2.1: pyridinium p-toluenesulfonate / methanol / 4 h / Reflux

3.1: pyridinium chlorochromate / dichloromethane / 16 h / 20 °C / Molecular sieve

4.1: dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3 h / 20 °C

5.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; tert-butyl alcohol; acetone / 20 h / 20 °C

5.2: 4 h / 20 °C

6.1: pyridine / 16 h / 20 °C

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

8.1: sodium hydroxide / ethanol; water / 12 h / 60 °C

9.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 20 °C

10.1: formic acid / diethyl ether / -5 °C

11.1: pyridinium chlorochromate / dichloromethane; diethyl ether / 20 °C / Molecular sieve

12.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / -70 °C

12.2: -70 - 20 °C

13.1: acetic acid; water / tetrahydrofuran / 20 °C

14.1: tetrahydrofuran; hexane / -70 °C

15.1: α,α,α-trifluorotoluene; magnesium oxide / 72 h / 85 °C

16.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 76 h / 20 °C

17.1: pyridine; dmap / 18 h / 20 °C / Cooling with ice

With pyridine; 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; formic acid; methanesulfonamide; α,α,α-trifluorotoluene; AD-mix-α; water; pyridinium p-toluenesulfonate; magnesium oxide; potassium hexamethylsilazane; acetic acid; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; toluene; tert-butyl alcohol; 12.1: |Wittig-Horner Reaction;
DOI:10.1271/bbb.120317 DOI:10.1271/bbb.120317