Technology Process of C31H44N4O3
There total 4 articles about C31H44N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ozone / methanol; dichloromethane / 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere
3.1: manganese(IV) oxide / benzene / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: pyridine; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere; solid phase reaction
4.2: 20 °C / Inert atmosphere; solid phase reaction
5.1: 5% Pd/Al2O3; hydrogen / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere
With
pyridine; manganese(IV) oxide; sodium tetrahydroborate; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine; 5% Pd/Al2O3; hydrogen; ozone;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; benzene;
DOI:10.1021/jm2007062
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere
2.1: manganese(IV) oxide / benzene / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: pyridine; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere; solid phase reaction
3.2: 20 °C / Inert atmosphere; solid phase reaction
4.1: 5% Pd/Al2O3; hydrogen / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere
With
pyridine; manganese(IV) oxide; sodium tetrahydroborate; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine; 5% Pd/Al2O3; hydrogen;
In
tetrahydrofuran; methanol; ethyl acetate; benzene;
DOI:10.1021/jm2007062
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: manganese(IV) oxide / benzene / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: pyridine; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere; solid phase reaction
2.2: 20 °C / Inert atmosphere; solid phase reaction
3.1: 5% Pd/Al2O3; hydrogen / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere
With
pyridine; manganese(IV) oxide; trityl chloride polystyrene resin; N,N-diethyl-N-isopropylamine; 5% Pd/Al2O3; hydrogen;
In
tetrahydrofuran; ethyl acetate; benzene;
DOI:10.1021/jm2007062