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Technology Process of C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

Base Information
  • Chemical Name:C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru
  • CAS No.:1298062-11-9
  • Molecular Formula:C46H46OP2Ru
  • Molecular Weight:777.888
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CCCH(OCH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)CH<sub>2</sub>CHCH<sub>2</sub>Ru

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Chemical Property of C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru
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Technology Process of C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

There total 1 articles about C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C<sub>5</sub>H<sub>5</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CCHCH(OCH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)CH<sub>2</sub>CHCH<sub>2</sub>Ru

C5H5((C6H5)2PCH2CH2P(C6H5)2)CCHCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

C<sub>5</sub>H<sub>5</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CCCH(OCH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)CH<sub>2</sub>CHCH<sub>2</sub>Ru
1298062-11-9

C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

Guidance literature:
With K2CO3; In methanol; ruthenium complex in MeOH was treated with K2CO3, stirred at room temp. for 10 min; evapd. in vac., dissolved in ether, filtered through celite, evapd. in vac, elem. anal.;
DOI:10.1039/c0dt01551b

Reference yield:

tetrafluoroboric acid

tetrafluoroboric acid

C<sub>5</sub>H<sub>5</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CCCH(OCH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)CH<sub>2</sub>CHCH<sub>2</sub>Ru
1298062-11-9

C5H5((C6H5)2PCH2CH2P(C6H5)2)CCCH(OCH3)C(C6H5)(CH3)CH2CHCH2Ru

C<sub>5</sub>H<sub>5</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)RuC(OH)CHCHC(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)CH<sub>2</sub>CHCH<sub>2</sub>

C5H5((C6H5)2PCH2CH2P(C6H5)2)RuC(OH)CHCHC(C6H5)(CH3)CH2CHCH2

Guidance literature:
In diethyl ether; (N2); 54 % HBF4 in ether was added to soln. of ruthenium complex in ether, ether was added at 0°C; filtered, washed with ether, dried in vac., elem. anal.;
DOI:10.1039/c0dt01551b
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