N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

Base Information

Chemical Name:N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide
CAS No.:1449004-51-6
Molecular Formula:C₃₁H₂₇IN₄O₆S₂
Molecular Weight:742.615
Hs Code.:

Synonyms:

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Chemical Property of N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

Chemical Property:

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Technology Process of N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

There total 6 articles about N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1449004-51-6
N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux

2: acetone / 5 h / 20 °C

3: acetone / 20 °C

With thionyl chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3ob40236c

Reference yield:

: 63-74-1
sulfanilamide

: 1449004-51-6
N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / tetrahydrofuran; water

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

3: trifluoroacetic acid / dichloromethane / 20 °C

4: acetone / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c3ob40236c

Reference yield:

: C₂₈H₃₁N₃O₇S

: 1449004-51-6
N-(4-(N-(N-carbobenzoxy-L-phenylalanyl)sulfamoyl)-phenylcarbamothioyl)-4-iodobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: acetone / 20 °C

With trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1039/c3ob40236c