2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene

Base Information

Chemical Name:2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene
CAS No.:74832-24-9
Molecular Formula:C₂₃H₁₆O
Molecular Weight:309.371
Hs Code.:

2-deuteriated 1-benzoylnaphtho<de-2.3.4>tricyclo-<4.3.0.0<sup>2,9</sup>>nona-3,7-diene

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Chemical Property of 2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene

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Technology Process of 2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene

There total 7 articles about 2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72602-42-7
8-Benzoyl-9-deuterio-naphthobicyclo<3,2,2>nona-2,6,8-trien

: 74832-24-9
C₂₃H₁₅⁽²⁾HO

: 72315-83-4
C₂₃H₁₅⁽²⁾HO

: 74832-25-0
C₂₃H₁₅⁽²⁾HO

Guidance literature:: In various solvent(s); at -196.1 ℃; Irradiation;
DOI:10.1021/ja00536a056

Reference yield:

: 81060-96-0
1-phenyl-3-deuterioprop-2-yn-1-one

: 74832-24-9
2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / 24 h / 120 °C

2: 27 percent / NaBH₄ / methanol; H₂O / 1 h / 0 °C

3: 2.) pyridinium chlorochromate / 1.) benzophenone / 1.) benzene, irrad., 3 h; 2.) methylene dichloride, 0 deg C, 15 min.

With sodium tetrahydroborate; pyridinium chlorochromate; benzophenone; In methanol; water;
DOI:10.1016/S0040-4020(01)92372-5

Reference yield:

: 81060-97-1
8-benzoyl-9-deuterionaphthobicyclo<3.2.2>nona-2,6,8-triene

: 74832-24-9
2-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>nona-3,7-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / NaBH₄ / methanol; H₂O / 1 h / 0 °C

2: 2.) pyridinium chlorochromate / 1.) benzophenone / 1.) benzene, irrad., 3 h; 2.) methylene dichloride, 0 deg C, 15 min.

With sodium tetrahydroborate; pyridinium chlorochromate; benzophenone; In methanol; water;
DOI:10.1016/S0040-4020(01)92372-5