3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline

Base Information

• Chemical Name: 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline
• CAS No.: 80992-35-4
• Molecular Formula: C₁₁H₁₀Cl₄N₂O
• Molecular Weight: 328.025
• Mol file: 80992-35-4.mol

Synonyms:

Chemical Property of 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline

There total 6 articles about 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Pyrrolidin-1-yl-(2,3,4,5-tetrachloro-6-isocyanato-phenyl)-methanone (80992-34-3) → 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline (80992-35-4)

Guidance literature:

With moisture in air;

DOI:10.1039/P19810002884

Reference yield:

tetrachlorophthalic anhydride (117-08-8) → 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline (80992-35-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 70 percent / acetone

2: 96 percent / perchloric acid, acetic anhydride

3: 73 percent / sodium azide / H₂O; acetone

4: 100 percent / benzene / 0.33 h / Heating

5: 100 percent / moisture in air

With sodium azide; perchloric acid; moisture in air; acetic anhydride; In water; acetone; benzene;

DOI:10.1039/P19810002884

Reference yield:

tetrachloro-NN-diethylphthalamic acid (6310-29-8) → 3,4,5,6-tetrachloro-2-pyrrolidinocarbonylaniline (80992-35-4)

Guidance literature:

Multi-step reaction with 6 steps

1: recrystallisation

2: 70 percent / acetone

3: 96 percent / perchloric acid, acetic anhydride

4: 73 percent / sodium azide / H₂O; acetone

5: 100 percent / benzene / 0.33 h / Heating

6: 100 percent / moisture in air

With sodium azide; perchloric acid; moisture in air; acetic anhydride; In water; acetone; benzene;

DOI:10.1039/P19810002884

upstream raw materials:

Pyrrolidin-1-yl-(2,3,4,5-tetrachloro-6-isocyanato-phenyl)-methanone

tetrachlorophthalic anhydride

tetrachloro-NN-diethylphthalamic acid

4,5,6,7-tetrachloro-3-hydroxy-3-pyrrolidinophthalide