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Technology Process of Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3

Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3

Base Information
  • Chemical Name:Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3
  • CAS No.:319930-51-3
  • Molecular Formula:CF3O3S*C32H61ClNOOsP2
  • Molecular Weight:912.513
  • Hs Code.:
Os(CCHC<sub>6</sub>H<sub>5</sub>)Cl(H<sub>2</sub>O)(NHC(CH<sub>2</sub>)5)(P(CH(CH<sub>3</sub>)2)3)2<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=[Os(CCHC<sub>6</sub>H<sub>5</sub>)Cl(H<sub>2</sub>O)(NHC(CH<sub>2</sub>)5)(P(CH(CH<sub>3</sub>)2)3)2]CF<sub>3</sub>SO<sub>3</sub>

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Chemical Property of Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3
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Technology Process of Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3

There total 1 articles about Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

[Os((E)-CHCHPh)Cl(NC(CH<sub>2</sub>)5)(P(i-Pr)3)2]CF<sub>3</sub>SO<sub>3</sub>
319930-43-3

[Os((E)-CHCHPh)Cl(NC(CH2)5)(P(i-Pr)3)2]CF3SO3

water
7732-18-5

water

Os(CCHC<sub>6</sub>H<sub>5</sub>)Cl(H<sub>2</sub>O)(NHC(CH<sub>2</sub>)5)(P(CH(CH<sub>3</sub>)2)3)2<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=[Os(CCHC<sub>6</sub>H<sub>5</sub>)Cl(H<sub>2</sub>O)(NHC(CH<sub>2</sub>)5)(P(CH(CH<sub>3</sub>)2)3)2]CF<sub>3</sub>SO<sub>3</sub>
319930-51-3

Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2(1+)*CF3SO3(1-)=[Os(CCHC6H5)Cl(H2O)(NHC(CH2)5)(P(CH(CH3)2)3)2]CF3SO3

Guidance literature:
In tetrahydrofuran; with exclusion of air, 1 equiv. of H2O was added to THF soln. of Os-complex at -20 °C, mixt. was kept. at this temp. for 3 days; soln. was evapd. to dryness at -20 °C, cold Et2O was added, solidwas washed 3 times with Et2O, dried in vac., elem. anal.;
DOI:10.1021/om0005295
upstream raw materials:

[Os((E)-CHCHPh)Cl(NC(CH2)5)(P(i-Pr)3)2]CF3SO3

water

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