10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

Base Information

Chemical Name:10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)
CAS No.:145089-55-0
Molecular Formula:C₃₀H₅₀N₅O₇P₃
Molecular Weight:685.678
Hs Code.:

Synonyms:

Suppliers and Price of 10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

There total 2 articles about 10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148932-45-0
triethyl 10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinate)

: 145089-55-0
10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

Guidance literature:: With potassium deuteroxide; In water-d2; for 16h; Ambient temperature;

Reference yield:

: 148932-44-9
1-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane

: 145089-55-0
10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 4 Angstroem molecular sieves / tetrahydrofuran / 18 h / Heating

2: KOD / D₂O / 16 h / Ambient temperature

With potassium deuteroxide; 4 A molecular sieve; In tetrahydrofuran; water-d2;

Reference yield:

: gadolinium(III) oxide

: 145089-55-0
10-(dibenzylcarbamoylmethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyltrimethylenetri(methylphosphinic acid)

: (C₈H₁₆N₄(CH₂P(CH₃)O₂)3(CH₂CON(CH₂C₆H₅)2))Gd

Guidance literature:: With sodium hydroxide; In not given; heating at pH 2, 80°C, 3h; raising pH to 6 (NaOH); chromy. (alumina, 10% methanol/CH2Cl2);
DOI:10.1039/c39920001441