C₆₆H₇₄F₈O₂Si₂

Base Information

Chemical Name:C₆₆H₇₄F₈O₂Si₂
CAS No.:1391865-47-6
Molecular Formula:C₆₆H₇₄F₈O₂Si₂
Molecular Weight:1107.47
Hs Code.:

C<sub>66</sub>H<sub>74</sub>F<sub>8</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₆H₇₄F₈O₂Si₂

Chemical Property:

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Technology Process of C₆₆H₇₄F₈O₂Si₂

There total 3 articles about C₆₆H₇₄F₈O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1167987-18-9
tri-cyclohexylsilyl acetylene

: 1391865-44-3
1,2,3,4,9,10,11,12-octafluorohexacene-6,15-dione

: 1391865-47-6
C₆₆H₇₄F₈O₂Si₂

Guidance literature:: tri-cyclohexylsilyl acetylene; With n-butyllithium; In hexane; at 0 ℃; for 1h; Inert atmosphere;

1,2,3,4,9,10,11,12-octafluorohexacene-6,15-dione; In tetrahydrofuran; hexane; for 3h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; Inert atmosphere;
DOI:10.1039/c2cc33919f

Reference yield:

: 1312175-99-7
[5,6,7,8-tetrafluoro-3-(hydroxymethyl)naphthalen-2-yl]methanol

: 1391865-47-6
C₆₆H₇₄F₈O₂Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; ethanol; water

3.1: n-butyllithium / hexane / 1 h / 0 °C / Inert atmosphere

3.2: 3 h / Inert atmosphere

3.3: Inert atmosphere

With n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; sodium hydroxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1039/c2cc33919f

Reference yield:

: 137676-39-2
dimethyl 5,6,7,8-tetrafluoronaphthalene-2,3-dicarboxylate

: 1391865-47-6
C₆₆H₇₄F₈O₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sodium hydroxide / tetrahydrofuran; ethanol; water

4.1: n-butyllithium / hexane / 1 h / 0 °C / Inert atmosphere

4.2: 3 h / Inert atmosphere

4.3: Inert atmosphere

With n-butyllithium; oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; sodium hydroxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1039/c2cc33919f