C₅₆H₆₆F₄N₈O₁₇

Base Information

Chemical Name:C₅₆H₆₆F₄N₈O₁₇
CAS No.:173325-30-9
Molecular Formula:C₅₆H₆₆F₄N₈O₁₇
Molecular Weight:1199.18
Hs Code.:

C<sub>56</sub>H<sub>66</sub>F<sub>4</sub>N<sub>8</sub>O<sub>17</sub>

Synonyms:

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Chemical Property of C₅₆H₆₆F₄N₈O₁₇

Chemical Property:

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Technology Process of C₅₆H₆₆F₄N₈O₁₇

There total 9 articles about C₅₆H₆₆F₄N₈O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 173193-15-2
(2R,5S)-5-(3-chloro-2-oxopropyl)-2-trichloromethyl-1,3-dioxolan-4-one

: 173325-30-9
C₅₆H₆₆F₄N₈O₁₇

Guidance literature:: Multi-step reaction with 8 steps

1: 86 percent / NaN₃, Et₄NBr / CH₂Cl₂; acetonitrile / 3 h / 0 °C

2: 56 percent / Zn(BH₄)2 / tetrahydrofuran; diethyl ether / 2 h / -10 °C

3: 81 percent / Ag₂O / dimethylformamide / 3 h / Ambient temperature

4: 82 percent / HCl / 0.17 h / Ambient temperature

5: 77 percent / diethylaminosulfur trifluoride / benzene; pyridine / 1 h, RT; 2 h, 60 deg C

6: 99 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

7: N,N'-dicyclohexylcarbodiimide / ethyl acetate / 1 h / Ambient temperature

8: 632 mg / NaHCO₃ / tetrahydrofuran; H₂O / 1 h / Ambient temperature; pH ca. 8

With hydrogenchloride; sodium hydroxide; sodium azide; zinc(II) tetrahydroborate; diethylamino-sulfur trifluoride; tetraethylammonium bromide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; silver(l) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/S0008-6215(97)10080-5

Reference yield:

: (2R,5S)-5-(3-Diazo-2-oxo-propyl)-2-trichloromethyl-[1,3]dioxolan-4-one

: 173325-30-9
C₅₆H₆₆F₄N₈O₁₇

Guidance literature:: Multi-step reaction with 9 steps

1: HCl / diethyl ether / 0.5 h / Ambient temperature

2: 86 percent / NaN₃, Et₄NBr / CH₂Cl₂; acetonitrile / 3 h / 0 °C

3: 56 percent / Zn(BH₄)2 / tetrahydrofuran; diethyl ether / 2 h / -10 °C

4: 81 percent / Ag₂O / dimethylformamide / 3 h / Ambient temperature

5: 82 percent / HCl / 0.17 h / Ambient temperature

6: 77 percent / diethylaminosulfur trifluoride / benzene; pyridine / 1 h, RT; 2 h, 60 deg C

7: 99 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

8: N,N'-dicyclohexylcarbodiimide / ethyl acetate / 1 h / Ambient temperature

9: 632 mg / NaHCO₃ / tetrahydrofuran; H₂O / 1 h / Ambient temperature; pH ca. 8

With hydrogenchloride; sodium hydroxide; sodium azide; zinc(II) tetrahydroborate; diethylamino-sulfur trifluoride; tetraethylammonium bromide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; silver(l) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/S0008-6215(97)10080-5

Reference yield:

: 173193-16-3
(2R,5S)-5-(3-azido-2-oxopropyl)-2-trichloromethyl-1,3-dioxolan-4-one

: 173325-30-9
C₅₆H₆₆F₄N₈O₁₇

Guidance literature:: Multi-step reaction with 7 steps

1: 56 percent / Zn(BH₄)2 / tetrahydrofuran; diethyl ether / 2 h / -10 °C

2: 81 percent / Ag₂O / dimethylformamide / 3 h / Ambient temperature

3: 82 percent / HCl / 0.17 h / Ambient temperature

4: 77 percent / diethylaminosulfur trifluoride / benzene; pyridine / 1 h, RT; 2 h, 60 deg C

5: 99 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

6: N,N'-dicyclohexylcarbodiimide / ethyl acetate / 1 h / Ambient temperature

7: 632 mg / NaHCO₃ / tetrahydrofuran; H₂O / 1 h / Ambient temperature; pH ca. 8

With hydrogenchloride; sodium hydroxide; zinc(II) tetrahydroborate; diethylamino-sulfur trifluoride; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; silver(l) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0008-6215(97)10080-5