C₂₆H₃₅N₅O₃Si

Base Information

Chemical Name:C₂₆H₃₅N₅O₃Si
CAS No.:1557248-91-5
Molecular Formula:C₂₆H₃₅N₅O₃Si
Molecular Weight:493.681
Hs Code.:

C<sub>26</sub>H<sub>35</sub>N<sub>5</sub>O<sub>3</sub>Si

Synonyms:

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Chemical Property of C₂₆H₃₅N₅O₃Si

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Technology Process of C₂₆H₃₅N₅O₃Si

There total 7 articles about C₂₆H₃₅N₅O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1557247-82-1
1-((2-(trimethylsilyl)ethoxy)methyl)-1,4,5,7-tetrahydrospiro[indazole-6,3'-oxetane]-3-carboxylic acid

: 28466-62-8
1-(phenylmethyl)-1H-pyrazol-4-amine

: 1557248-91-5
C₂₆H₃₅N₅O₃Si

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm500550e

Reference yield:

: 1557247-85-4
ethyl 2-diazo-2-(7-hydroxy-2-oxaspiro[3.5]nonan-7-yl)acetate

: 1557248-91-5
C₂₆H₃₅N₅O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 0.25 h

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.2: 0 - 20 °C

3.1: lithium hydroxide monohydrate / acetonitrile; water; tetrahydrofuran / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With lithium hydroxide monohydrate; sodium hydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm500550e

Reference yield:

: 2-oxaspiro[3.5]nonan-7-one

: 1557248-91-5
C₂₆H₃₅N₅O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 0.25 h

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

3.2: 0 - 20 °C

4.1: lithium hydroxide monohydrate / acetonitrile; water; tetrahydrofuran / 20 °C

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With n-butyllithium; lithium hydroxide monohydrate; sodium hydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm500550e