fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3

Base Information

• Chemical Name: fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3
• CAS No.: 83828-75-5
• Molecular Formula: C₃₀H₂₇N₃O₃W
• Molecular Weight: 661.413

Synonyms:

Chemical Property of fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3

There total 2 articles about fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tungsten hexacarbonyl (14040-11-0) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3 (83828-75-5)

Guidance literature:

palladium(II) oxide; In toluene; Protective gas (Ar), refluxing.; Recrystn. (hexane/dichloromethane).;

Reference yield:

tungsten hexacarbonyl (14040-11-0) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3 (83828-75-5) + tungsten pentacarbonyl 2,6-dimethylphenyl isocyanide (76374-92-0) + cis-tungsten tetracarbonyl (2,6-dimethylphenyl isocyanide)2 (83808-57-5)

Guidance literature:

palladium(II) oxide; In benzene; refluxed;

DOI:10.1016/S0020-1693(00)93476-5

Reference yield:

fac-tungsten tricarbonyl (2,6-dimethylphenyl isocyanide)3 (83828-75-5) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → tungsten carbonyl (2,6-dimethylphenyl isocyanide)5 (83828-76-6)

Guidance literature:

palladium(II) oxide; In toluene; refluxed for 3 h;

DOI:10.1016/S0020-1693(00)93476-5

upstream raw materials:

tungsten hexacarbonyl

2,6-dimethylphenyl isonitrile

Downstream raw materials:

tungsten carbonyl (2,6-dimethylphenyl isocyanide)5

tungsten (2,6-dimethylphenyl isocyanide)6

W(CO)2((CH₃)2C₆H₃NC)3I₂

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