(+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

Base Information

Chemical Name:(+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine
CAS No.:470670-87-2
Molecular Formula:C₂₅H₂₂N₂O₆S
Molecular Weight:478.525
Hs Code.:

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Chemical Property of (+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

Chemical Property:

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Technology Process of (+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

There total 4 articles about (+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 470670-88-3
(+/-)-methyl-N-benzyloxycarbonyl-1-tosyl-3-indoleglycinate

: 470670-87-2,470670-89-4
(+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

Guidance literature:: With potassium hydroxide; water; In 1,4-dioxane; at 20 ℃; for 0.5h;
DOI:10.1021/ol026660l

Reference yield:

: 6747-15-5
α-amino-(+/)-3-indoleacetic acid

: 470670-87-2,470670-89-4
(+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaOH / H₂O / cooling

1.2: NaOH / H₂O / 0.5 h / 20 °C

2.1: 2.3 g / K₂CO₃ / dimethylformamide / 4 h / 20 °C

3.1: 76 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂ / -20 °C

4.1: 98 percent / KOH; H₂O / dioxane / 0.5 h / 20 °C

With potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; water; potassium carbonate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol026660l

Reference yield:

: 294888-41-8
(+/-)-N-benzyloxycarbonyl-3-indoleglycinate

: 470670-87-2,470670-89-4
(+/-)-N-benzyloxycarbonyl-1-tosyl-3-indoleglycine

Guidance literature:: Multi-step reaction with 3 steps

1: 2.3 g / K₂CO₃ / dimethylformamide / 4 h / 20 °C

2: 76 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂ / -20 °C

3: 98 percent / KOH; H₂O / dioxane / 0.5 h / 20 °C

With potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; water; potassium carbonate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol026660l