(Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

Base Information

Chemical Name:(Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)
CAS No.:154676-86-5
Molecular Formula:C₃₆H₅₆P₂PdS₂
Molecular Weight:721.34
Hs Code.:

(Pd(S(C<sub>6</sub>H<sub>5</sub>))2(P(C<sub>6</sub>H<sub>11</sub>)2H)2)

Synonyms:

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Chemical Property of (Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

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Technology Process of (Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

There total 5 articles about (Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (Pd₂(P(C₆H₁₁)2)(C₃H₅)(P(C₆H₁₁)2H)2)

: 108-98-5
thiophenol

: 829-84-5
dicyclohexylphosphane

: 154676-86-5
(Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

Guidance literature:: In hexane; byproducts: propene, hydrogen; soln. of PCy2H and PhSH in hexane is added dropwise to soln. of the Pd compd. in hexane under nitrogen, solid started to ppt., mixt. is concd., acetone is added, mixt. is cooled to -30°C for 1 night; filtn., drying (vac.);

Reference yield: 60.0%

: (Pd₃(P(C₆H₁₁)2)2(S(C₆H₅))2(P(C₆H₁₁)2H)2)

: 108-98-5
thiophenol

: 829-84-5
dicyclohexylphosphane

: 154676-86-5
(Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

Guidance literature:: In toluene; byproducts: hydrogen; PCy2H and PhSH are added to a soln. of the Pd compd. in toluene under nitrogen, soln. is stirred at room temp. overnight; concn., acetone is added, mixt. is cooled at -30°C for 3 h, filtn., drying (vac.);

Reference yield: 47.0%

: [Pd2(μ-PCy2)(μ,η(3)-C3H5)(PCy2H)2]

: 108-98-5
thiophenol

: 154676-86-5
(Pd(S(C₆H₅))2(P(C₆H₁₁)2H)2)

Guidance literature:: In hexane; addn. of thiophenol (excess) to Pd complex soln. under N2, 20°C; keeping at room temp. overnight; crystn.; filtration; drying (vac.); elem. anal.; monitoring by 31P-NMR;