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Technology Process of HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2

HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2

Base Information
  • Chemical Name:HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2
  • CAS No.:1227178-20-2
  • Molecular Formula:C68H58Cl2HgN2O6P4
  • Molecular Weight:1394.61
  • Hs Code.:
HgCl<sub>2</sub>[(C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CHC(O)C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>]2

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Chemical Property of HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2
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Technology Process of HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2

There total 1 articles about HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

(C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CHC(O)C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>
1227178-18-8

(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2

mercury dichloride

mercury dichloride

HgCl<sub>2</sub>[(C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CHC(O)C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>]2
1227178-20-2

HgCl2[(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2]2

Guidance literature:
In methanol; under N2, using standard Schlenk technique; to MeOH soln. of HgCl2 addedMeOH soln. of ylide compd. dropwise at 0°C; stirred for 2 h; treated with CH2Cl2, filtered through celite; MeOH added; elem. anal.;
DOI:10.1016/j.ica.2010.01.024
upstream raw materials:

(C6H5)2PCH2CH2P(C6H5)2CHC(O)C6H4NO2

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