dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl

Base Information

• Chemical Name: dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl
• CAS No.: 264891-96-5
• Molecular Formula: C₃₆H₄₆OSiTi
• Molecular Weight: 570.726

Synonyms:

Chemical Property of dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl

There total 1 articles about dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dichloride + phenylmagnesium bromide (1589-82-8) → dimethylsilyl(2,3,4,5-tetramethylcyclopentadienyl)(3-tert-butyl-5-methyl-2-phenoxy)-titanium dibenzyl (264891-96-5)

Guidance literature:

In diethyl ether; (N2); std. Schlenk technique; soln. of Mg compd. in Et2O was added to mixt. of Ti complex in Et2O at -78°C; warmed to room temp.; stirredfor 3 h; solvent removed; hexane added; filtered; solvent removed; recrystd. (hexane); elem. anal.;

DOI:10.1016/j.jorganchem.2007.06.012

upstream raw materials:

phenylmagnesium bromide

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