(OC)5WC(OCH₃)C₆H₁₀OC₂H₅

Base Information

• Chemical Name: (OC)5WC(OCH₃)C₆H₁₀OC₂H₅
• CAS No.: 79542-87-3
• Molecular Formula: C₁₅H₁₈O₇W
• Molecular Weight: 494.154
• Mol file: 79542-87-3.mol

Synonyms:

Chemical Property of (OC)5WC(OCH₃)C₆H₁₀OC₂H₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (OC)5WC(OCH₃)C₆H₁₀OC₂H₅

There total 1 articles about (OC)5WC(OCH₃)C₆H₁₀OC₂H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

(methoxy(methyl)methylidene)pentacarbonyltungsten + 1-ethoxycyclohexene (1122-84-5) → (OC)5WC(OCH3)C6H10OC2H5 (79542-87-3)

Guidance literature:

With methyllithium; trifluoroacetic acid; In diethyl ether; complex/ether treated with 1 equiv of CH3Li at -40°C, 2 equiv oforg. educt added, 1 equiv of CF3CO2H added, reacted for 15 min; treated with NaHCO3, chromd. (SiO2, petroleum ether, ether/petroleum ether);

DOI:10.1016/S0022-328X(00)81917-8

Reference yield:

(OC)5WC(OCH3)C6H10OC2H5 (79542-87-3) → (OC)5WC(OCH3)CHC(CH2)5 (79542-81-7)

Guidance literature:

With aluminum oxide; In hexane; kept for 2 h; filtered;

DOI:10.1016/S0022-328X(00)81917-8

upstream raw materials:

1-ethoxycyclohexene

Downstream raw materials:

(OC)5WC(OCH₃)CHC(CH₂)5