PrCW(OBu(t))3

Base Information

Chemical Name:PrCW(OBu(t))3
CAS No.:82209-25-4
Molecular Formula:C₁₆H₃₄O₃W
Molecular Weight:458.294
Hs Code.:

Synonyms:

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Chemical Property of PrCW(OBu(t))3

Chemical Property:

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Technology Process of PrCW(OBu(t))3

There total 4 articles about PrCW(OBu(t))3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 57125-20-9
ditungsten hexa-tert-butoxide

: 18727-91-8
Ph₃SiCCPr

: 82209-25-4
PrCW(OBu(t))3

: tris(tert-butoxy)triphenylsilylmethylidinetungsten

Guidance literature:: In pentane; soln. Ph3SiCCPr in pentane was added to soln. W2(OBu(t))6 in pentane, 20°C, 1 h; pentane was removed, PrCW(OBu(t))3 was sublimed (85-90°C, 1E-2-1E-3 Torr, 1 h), residue was recrystd. from pentane - Ph3SiCW(OBu(t))3; elem. anal.;
DOI:10.1023/B:RUCB.0000011869.83994.94

Reference yield: 74.39%

: 57125-20-9
ditungsten hexa-tert-butoxide

: 5054-22-8
n-C₃H₇C₂Ge(C₆H₅)2C₂C₃H₇-n

: 82209-25-4
PrCW(OBu(t))3

: diphenyldi[tris(tert-butoxy)tungstenmethylidino]germane

Guidance literature:: In pentane; soln. Ph2Ge(CCPr)2 in pentane was added to soln. W2(OBu(t))6 in pentane,20°C, 30 min; pentane was removed, PrCW(OBu(t))3 was sublimed (85-90°C, 1E-2-1E-3 Torr, 1 h), residue was recrystd. from pentane - Ph3SiCW(OBu(t))3; elem. anal.;
DOI:10.1023/B:RUCB.0000011869.83994.94

Reference yield: 69.97%

: 57125-20-9
ditungsten hexa-tert-butoxide

: 728007-05-4
Ph₂Sn(CCPr)2

: 82209-25-4
PrCW(OBu(t))3

: diphenyldi[tris(tert-butoxy)tungstenmethylidino]stannane

Guidance literature:: In pentane; soln. Ph2Sn(CCPr)2 in pentane was added to soln. W2(OBu(t))6 in pentane,20°C, 30 min; pentane was removed, PrCW(OBu(t))3 was sublimed (85-90°C, 1E-2-1E-3 Torr, 1 h), residue was recrystd. from pentane - Ph3SiCW(OBu(t))3; elem. anal.;
DOI:10.1023/B:RUCB.0000011869.83994.94