Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))

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Chemical Name:Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))
CAS No.:37048-02-5
Molecular Formula:C₄₄H₂₈FeN₄*Na
Molecular Weight:691.57
Hs Code.:

Na<sup>(1+)</sup>*Fe(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)4)<sup>(1-)</sup>=Na(Fe(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)4))

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Chemical Property of Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))

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Technology Process of Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))

There total 1 articles about Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 12582-61-5
μ-oxo-bis[α,β,γ,δ-tetraphenylporphinatoiron]

: 37048-02-5
Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))

Guidance literature:: With sodium amalgam; In toluene; a toluene soln. of Fe-complex was added under inert atmosphere to a suspn. of Na amalgam in toluene, mixt. was heated under reflux; ppt. was sepd. by filtration, extd. with 5:1 Et2O/benzene, this soln. was used for further reactions;
DOI:10.1016/0022-328X(83)80109-0

Reference yield:

: 37048-02-5
Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₅)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₅)4))

: 79197-95-8
(tetraphenylporphyrin)Fe(CH₃)

Guidance literature:: With methyl iodide; In diethyl ether; benzene; an excess of MeI was added dropwise with vigorous stirring to a soln. of Fe(I)-complex in 5:1 benzene/Et2O at ambient temp. under inert atmosphere, mixt. was stirred for several min (UV-vis monitoring); solvent was evapd., residue recrystd. from benzene-heptane; identified by the comparison of spectral data with that of authentic sample;
DOI:10.1016/0022-328X(83)80109-0