tris(4-tert-butylphenoxo)oxovanadium(V)

Base Information

Chemical Name:tris(4-tert-butylphenoxo)oxovanadium(V)
CAS No.:152845-83-5
Molecular Formula:C₃₀H₃₉O₄V
Molecular Weight:514.579
Hs Code.:

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Chemical Property of tris(4-tert-butylphenoxo)oxovanadium(V)

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Technology Process of tris(4-tert-butylphenoxo)oxovanadium(V)

There total 1 articles about tris(4-tert-butylphenoxo)oxovanadium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: vanadium(V) oxytrichloride

: 25237-79-0
(4-tert-butylphenoxy)trimethylsilane

: 152845-83-5
tris(4-tert-butylphenoxo)oxovanadium(V)

Guidance literature:: In tetrachloromethane; byproducts: (CH3)3SiCl; reaction of trimethyl-4-t-butylphenoxide with ice-cooled VOCl3 in CCl4 under anhyd. conditions, stirring for 4-5 h, colour changes from purple to reddish brown; distn. of Me3SiCl and excess solvent, drying under vacuum, elem. anal.;

Reference yield: 86.0%

: 152845-83-5
tris(4-tert-butylphenoxo)oxovanadium(V)

: 108-18-9
diisopropylamine

: 152680-33-6
bis(diisopropylamine)tris(4-tert-butylphenoxo)oxovanadium(V)

Guidance literature:: In tetrachloromethane; reaction of V-compd. with amine in 1:2 molar ratio in carbon tetrachloride, colour changes on addn. of the base, refluxing for about 2-3 h with stirring; slight concn., leaving overnight, pptn., recrystn. from n-hexane/CH2Cl2, drying under vacuum, elem. anal.;

Reference yield: 85.0%

: 152845-83-5
tris(4-tert-butylphenoxo)oxovanadium(V)

: 109-73-9,85404-21-3
N-butylamine

: 152680-30-3
bis(n-butylamine)tris(4-tert-butylphenoxo)oxovanadium(V)

Guidance literature:: In tetrachloromethane; reaction of V-compd. with amine in 1:2 molar ratio in carbon tetrachloride, colour changes on addn. of the base, refluxing for about 2-3 h with stirring; slight concn., leaving overnight, pptn., recrystn. from n-hexane/CH2Cl2, drying under vacuum, elem. anal.;