(3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II)

Base Information

• Chemical Name: (3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II)
• CAS No.: 339557-03-8
• Molecular Formula: C₂₀H₁₉CoNO₄
• Molecular Weight: 396.368
• Mol file: 339557-03-8.mol

Synonyms:

Chemical Property of (3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II)

There total 1 articles about (3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

bis-acetylacetonatocobalt(II) dihydrate + 1-{3-[(2-hydroxy-3-methoxy-benzylidene)-amino]-phenyl}-ethanone (788-18-1) → (3-acetophenylsalicylaldiminato)acetylacetonato cobalt(II) (339557-03-8) + bis-(3-acetophenylsalicylaldiminato)acetylacetonato cobalt(III) (339557-01-6)

Guidance literature:

With air; In ethanol; Co-contg. compd. (4 mmol) in ethanol was added to ethanolic soln. of a ligand (8 mmol); the mixt. was stirred at room temp. for 2 h; reflux for 3 h; column chromy. (silica gel; elution with ethanol); the first fraction, on removal of the solvent, was washed with diethyl ether and dried in vac.; recrystn. from CH2Cl2-n-hexane; the same treatment was for the middlefraction; elem. anal.;

upstream raw materials:

1-{3-[(2-hydroxy-3-methoxy-benzylidene)-amino]-phenyl}-ethanone