racemic 1-benzyloxy-3-butylamine

Base Information

• Chemical Name: racemic 1-benzyloxy-3-butylamine
• CAS No.: 340775-25-9
• Molecular Formula: C₁₁H₁₇NO
• Molecular Weight: 179.262
• Mol file: 340775-25-9.mol

Synonyms:

Chemical Property of racemic 1-benzyloxy-3-butylamine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of racemic 1-benzyloxy-3-butylamine

There total 1 articles about racemic 1-benzyloxy-3-butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

SEC-BUTYLAMINE (33966-50-6) + benzyl alcohol (100-51-6,185532-71-2) → racemic 1-benzyloxy-3-butylamine (340775-25-9)

Guidance literature:

SEC-BUTYLAMINE; benzyl alcohol; With 2-hydroxy-3-pyridinecarboxaldehyde; palladium diacetate; 1-fluoro-2,4,6-trimethylpyridin-1-ium tetrafluoroborate; at 70 ℃;

With N-methoxylamine hydrochloride; triethylamine;

DOI:10.1021/acscatal.0c01310

Reference yield:

racemic 1-benzyloxy-3-butylamine (340775-25-9) → (R)-1-benzyloxy-3-butylamine (340775-26-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / isopropyl alcohol; water / 40 °C / Reflux

2: sodium hydroxide / water / pH 13

With acetic acid; sodium hydroxide; In water; isopropyl alcohol;

upstream raw materials:

SEC-BUTYLAMINE

benzyl alcohol

Downstream raw materials:

(R)-1-benzyloxy-3-butylamine