C₁₅H₂₂INO₂

Base Information

• Chemical Name: C₁₅H₂₂INO₂
• CAS No.: 1401709-86-1
• Molecular Formula: C₁₅H₂₂INO₂
• Molecular Weight: 375.25
• Mol file: 1401709-86-1.mol

Synonyms:

Chemical Property of C₁₅H₂₂INO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₅H₂₂INO₂

There total 1 articles about C₁₅H₂₂INO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

octyl ester of p-aminobenzoic acid (14309-41-2) → C15H22INO2 (1401709-86-1)

Guidance literature:

With iodine; silver sulfate; In ethanol; at 20 ℃;

DOI:10.1039/c2cc35743g

Reference yield:

bis(trichloromethyl) carbonate (32315-10-9) + C15H22INO2 (1401709-86-1) → C31H42I2N2O5 (1401709-90-7)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃;

DOI:10.1039/c2cc35743g

Reference yield:

C15H22INO2 (1401709-86-1) → C41H56N2O7 (1401709-99-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane; water / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / tetrahydrofuran / 19 h / 55 - 58 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; 2: |Sonogashira Cross-Coupling;

DOI:10.1039/c2cc35743g

upstream raw materials:

octyl ester of p-aminobenzoic acid

Downstream raw materials:

C₃₁H₄₂I₂N₂O₅

C₄₁H₅₆N₂O₇