η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate

Base Information

Chemical Name:η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate
CAS No.:852415-02-2
Molecular Formula:C₁₈H₁₄Br₂ClFeO*F₆P
Molecular Weight:642.381
Hs Code.:

Synonyms:

Suppliers and Price of η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate

There total 1 articles about η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: η-cyclopentadienyl-η-1,4-dichlorobenzeneiron(II) hexafluorophosphate

: 13979-81-2
3,5-dibromo-4-methylphenol

: 852415-02-2
η6-[1-chloro-4-(3,5-dibromo-4-methylphenoxy)benzene]-η5-cyclopentadienyliron(II) hexafluorophosphate

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; (N2); phenol was stirred with NaH/mineral oil in THF for 15-20 min; soln. was added dropwise to stirred suspn. of Fe complex in THF at -78°C; mixt. was warmed to 0°C and stirred for 3 h; few drops of H2O added; passed through Celite, which subsequently washedwith CH2Cl2; solvent removed (vac.); redissolved in CH2Cl2; washed (NH4 PF6, NaOH, H2O); org. layer dried (MgSO4); solvent removed (vac.); residue triturated with ether; elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.032