Technology Process of C62H58N4(2-)
There total 9 articles about C62H58N4(2-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C / Inert atmosphere
1.2: 0.5 h / 0 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Inert atmosphere
2.2: 8 h / Inert atmosphere; Reflux
3.1: tetrabutylammonium borohydride / dichloromethane
With
n-butyllithium; sodium hydride; tetrabutylammonium borohydride;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; mineral oil;
DOI:10.1021/ja206060n
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C
2.1: aluminum oxide; copper(ll) bromide / tetrachloromethane / 85 °C
3.1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C / Inert atmosphere
3.2: 0.5 h / 0 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Inert atmosphere
4.2: 8 h / Inert atmosphere; Reflux
5.1: tetrabutylammonium borohydride / dichloromethane
With
aluminum oxide; n-butyllithium; boron trifluoride diethyl etherate; sodium hydride; tetrabutylammonium borohydride; copper(ll) bromide;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; hexane; dichloromethane; mineral oil;
DOI:10.1021/ja206060n
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: naphthalene; lithium / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
1.2: 0.5 h / 20 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C
3.1: aluminum oxide; copper(ll) bromide / tetrachloromethane / 85 °C
4.1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C / Inert atmosphere
4.2: 0.5 h / 0 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Inert atmosphere
5.2: 8 h / Inert atmosphere; Reflux
6.1: tetrabutylammonium borohydride / dichloromethane
With
aluminum oxide; n-butyllithium; naphthalene; boron trifluoride diethyl etherate; lithium; sodium hydride; tetrabutylammonium borohydride; copper(ll) bromide;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; hexane; dichloromethane; mineral oil;
DOI:10.1021/ja206060n